Hot-working

The HAYNES® and HASTELLOY® alloys can be hot-worked into various shapes; however, they can be more sensitive to the amounts and rates of hot-reduction than the austenitic stainless steels. In addition, the hot-working temperature ranges for the HAYNES® and HASTELLOY® alloys are quite narrow, and careful attention to hot-working parameters is necessary

In developing suitable hot-working practices, particular attention should be paid to the solidus of the alloy in question (the temperature at which the alloy begins to melt), the high strengths of the HAYNES® and HASTELLOY® alloys at elevated temperatures, their high work-hardening rates, and their low-thermal conductivities. Furthermore, their resistance to deformation increases markedly as the temperature falls to the low end of the hot-working range.

Accordingly, hot-working practices that incorporate high (heavy) initial reductions, followed by moderate final reductions, coupled with frequent re-heating, generally yield the best results. In addition, slow deformation rates tend to minimize adiabatic heating and applied force requirements.

*Following any hot-working operation, the HAYNES® and HASTELLOY® alloys should be annealed, to return them to their optimal condition for service, age-hardening (in the case of the age-hardenable alloys), or for further fabrication. Annealing temperatures and techniques are detailed in the heat treatment section.

Melting Temperature Ranges

Melting Temperature Range
Alloy Solidus* Liquidus**
- °F °C °F °C
B-3® 2500 1370 2585 1418
C-4 - -
C-22® 2475 1357 2550 1399
C-22HS® 2380 1304 2495 1368
C-276 2415 1323 2500 1371
C-2000® 2422 328 2476 1358
G-30® - -
G-35® 2430 1332 2482 1361
HYBRID-BC1® 2448 1342 2509 1376
N 2375 1302 2550 1399
ULTIMET® 2430 1332 2470 1354
25 2425 1329 2570 1410
75 2445 1341 2515 1379
188 2400 1316 2570 1410
214® 2475 1357 2550 1399
230® 2375 1302 2500 1371
242® 2350 1288 2510 1377
244® 2480 1360 2550 1399
263 2370 1299 2470 1354
282® 2370 1299 2510 1377
556® 2425 1329 2480 1360
617 2430 1332 2510 1377
625 2350 1288 2460 1349
625SQ® 2350 1288 2460 1349
718 2300 1260 2435 1335
HR-120® 2478 1359 2542 1395
HR-160® 2360 1293 2500 1371
HR-224® 2449 1343 2510 1377
HR-235® 2401 1316 2473 1356
MULTIMET® 2350 1288 2470 1354
R-41 2385 1307 2450 1343
S 2435 1335 2516 1380
W 2350 1288 2510 1377
Waspaloy 2425 132 2475 1357
X 2300 1260 2470 1354
X-750 2540 1393 2600 1427

*Temperature at which alloy starts to melt
**Temperature at which alloy is fully molten

Forging

Recommended Procedures and Temperatures Applicable to:
Corrosion-resistant Alloys
High-temperature Alloys
Wear & Corrosion-resistant Alloy

The following procedures are recommended for forging of the HAYNES® and HASTELLOY® alloys:

  • Soak billets or ingots at the forging start temperature for at least 30 minutes per inch of thickness. The use of a calibrated optical pyrometer is essential.
  • The stock should be turned frequently to make sure that it is heated evenly. Direct flame impingement on the alloy must be avoided.
  • Forging should begin immediately after withdrawal from the furnace. A short time lapse may allow surface temperatures to drop as much as 100-200°F (55-110°C). Do not raise the forging temperature to compensate for heat loss, as this may cause incipient melting.
  • Moderately heavy reductions (25-40%) are beneficial, to maintain as much internal heat as possible, thus minimizing grain coarsening and the number of re-heatings. Reductions greater than 40% per pass should be avoided.
  • Care must be taken to impart sufficient hot-work during forging to ensure that the appropriate structure and properties are achieved in the final part. For parts with large cross-sections, it is advisable to include a number of forging upsets in the hot-working schedule, to allow for adequate forging reductions. Upset L/D ratios of 3:1 are generally acceptable.
  • Light-reduction finish sizing sessions should generally be avoided. If required, they should be performed at the lower end of the forging temperature range.
  • Do not make radical changes in the cross-sectional shape, such as going directly from a square to a round, during initial forming stages. Instead, go from a square to a “round cornered square”, then to an octagon, then to a round.
  • Remove (condition) any cracks or tears developed during forging. This can be done at intermediate stages, between forging sessions.

Forging/Hot-working Temperature Ranges

Forging/Hot-Working Temperature
Alloy Start Temperature* Finish Temperature**
- °F °C °F °C
B-3® 2275 1246 1750 954
C-4 2200 1204 1750 954
C-22® 2250 1232 1750 954
C-22HS® 2250 1232 1750 954
C-276 2250 1232 1750 954
C-2000® 2250 1232 1750 954
G-30® 2200 1204 1800 982
G-35® 2200 1204 1750 954
HYBRID-BC1® 2250 1232 -
N 2200 1204 1750 954
ULTIMET® 2200 1204 1750 954
25 2200 1204 1750 954
75 2200 1204 1700 927
188 2150 1177 1700 927
214® 2150 1177 1800 982
230® 2200 1204 1700 927
242® 2125 1163 1750 954
244® - -
263 2150 1177 1750 954
282® 2125 1163 1850 1010
556® 2150 1177 1750 954
617 2125 1163 1600 871
625 2150 1177 1600 871
625SQ® - -
718 2050 1121 1650 899
HR-120® 2150 1177 1700 927
HR-160® 2050 1121 1600 871
HR-224® - -
HR-235® 2250 1232 1750 954
MULTIMET® 2150 1177 1700 927
R-41 2150 1177 1850 1010
S 2100 1149 1700 927
W 2240 1227 1800 982
Waspaloy 2150 1177 1850 1010
X 2100 1149 1750 954
X-750 2150 1177 1750 954

*Maximum
**Dependent upon the nature and degree of working

Hot-rolling

Recommended Procedures and Temperatures Applicable to:
Corrosion-resistant Alloys
High-temperature Alloys
Wear & Corrosion-resistant Alloy

Hot rolling of the HAYNES® and HASTELLOY® alloys can be performed to produce conventional rolled forms, such as bars, rings, and flats. The hot rolling temperature range is the same as that listed above (in the Forging section, under Forging/Hot-working Temperature Ranges).

Moderate reductions per pass (15 to 20 percent reduction in area), and rolling speeds of 200 to 300 surface feet per minute tend to provide good results, without overloading the mill. The total reduction per session should be at least 20 to 30 percent. It is usual to finish at the low end of the hot-working temperature range, since this generally provides the optimum structure and properties.

Care should be taken to ensure that the work piece is thoroughly soaked at the hot working start temperature before rolling. Frequent re-heating may be required during hot-rolling, to keep the temperature of the work piece in the hot working range.

Hot-forming

Recommended Procedures and Temperatures Applicable to:
Corrosion-resistant Alloys
High-temperature Alloys
Wear & Corrosion-resistant Alloy

The hot-forming of plates into components, such as dished heads is normally performed by cold-pressing or spinning, with intermediate anneals. However, sometimes the size and thickness of the material is such that hot-forming is necessary.

When hot-forming is required, the start temperature (to which the furnace is heated) is approximately mid-way between the annealing temperature (of the alloy in question) and its lower (finish) forging temperature. During hot-forming, the temperature of the piece should not fall below the lower (finish) forging temperature. Re-heating may be necessary to maintain the correct hot forming temperature, and dies should be warmed to avoid excessive chilling of the surfaces.

Other Hot-Working Processes

Recommended Procedures and Temperatures Applicable to:
Corrosion-resistant Alloys
High-temperature Alloys
Wear & Corrosion-resistant Alloy

The HAYNES® and HASTELLOY® alloys are amenable to several other hot-working processes, such as hot-extrusion and hot-spinning. Impact extrusion should be performed at the solution annealing temperature of the alloy involved. Uniform and accurate temperatures throughout the work-piece are necessary during impact extrusion, and re-strikes should be avoided. The parameters for hot extrusion and hot spinning are specific to the exact nature of the intended work and material. For more information, please contact our technical support team.